Synthesis and Crystal Structure of 1-(3-fluorophenyl)-3-(3,4,5-trimethoxybenzoyl)thiourea
The title thiourea was synthesized by reaction of 3,4,5-trimethoxybenzoyl isothiocyante with 3-fluoroaniline. The 3,4,5-trimethoxybenzoyl isothiocyante was produced in situ by reaction of 3,4,5-trimethoxybenzoyl chloride with ammonium thiocyanate in dry acetonitrile. The structure was confirmed by the spectroscopic, elemental analysis and single crystal X-ray diffraction data. It crystallizes in the monoclinic space group P21/c with unit cell dimensions a = 13.0966(9), b = 16.6460(13), c = 7.8448(5), β = 106.721(5)°, V 1637.9(2) ų, Z = 4.
| Author: | Aamer Saeed, Uzma Shaheen, Michael Bolte |
|---|---|
| URN: | urn:nbn:de:hebis:30:3-252688 |
| DOI: | http://dx.doi.org/10.3390/cryst1020034 |
| ISSN: | 2073-4352 |
| Parent Title (English): | Crystals |
| Publisher: | Molecular Diversity Preservation International (MDPI) |
| Place of publication: | Basel |
| Document Type: | Article |
| Language: | English |
| Date of Publication (online): | 09.05.2011 |
| Date of first Publication: | 09.05.2011 |
| Publishing Institution: | Univ.-Bibliothek Frankfurt am Main |
| Tag: | 1-(3-fluorophenyl)-3-(3,4,5-trimethoxybenzoyl)thiourea; Synthesis; crystal structure |
| Volume: | 1.2011 |
| Issue: | 2 |
| Pagenumber: | 6 |
| First Page: | 34 |
| Last Page: | 39 |
| Institutes: | Biochemie und Chemie |
| Dewey Decimal Classification: | 540 Chemie und zugeordnete Wissenschaften |
| Sammlungen: | Universitätspublikationen |
| Licence (German): |  Creative Commons - Namensnennung 3.0 |
